Hollow cone dark field imaging: automatic acquisition, and its contrast for magnesium

dc.contributor.authorParsa, Farhang
dc.contributor.examiningcommitteeLiang, Xihui (Mechanical Engineering)
dc.contributor.examiningcommitteeGuyot, Meghan (Mechanical Engineering)
dc.contributor.supervisorZhu, Guozhen
dc.date.accessioned2025-06-02T17:02:19Z
dc.date.available2025-06-02T17:02:19Z
dc.date.issued2025-05-27
dc.date.submitted2025-05-27T19:15:10Zen_US
dc.degree.disciplineMechanical Engineering
dc.degree.levelMaster of Science (M.Sc.)
dc.description.abstractHollow Cone Dark Field (HCDF) imaging is a powerful technique, yet it remains under-used for contrast-orientation studies—particularly when rapid, well-timed illumination adjustments are required and, up to the present time of authoring this thesis, no dedicated simulation protocols exist. The key obstacle is software fragmentation: conical-illumination simulation, beam-tilt control, automatic acquisition, and quantitative validation reside in separate programs. Researchers must therefore stitch together ad-hoc scripts and file conversions, hampering usability, reproducibility, and high-throughput studies. This study addresses the challenge by presenting a single, automated framework that unifies the entire HCDF workflow. A common scripting layer (i) generates orientation grids and supercells, (ii) performs multi-slice simulations, (iii) drives the microscope through continuous hollow-cone tilts while capturing images autonomously, and (iv) overlays experimental and simulated patterns with full parameter logging—eliminating manual data hand-offs at every stage. Demonstrated on magnesium crystals, the system simulates several hundred HCDF images, with experimental contrast matching simulation closely enough to validate both model and instrument settings. By fusing simulation, real-time acquisition, and validation into one cohesive environment, the framework transforms HCDF from a specialist method into a practical, high-throughput technique helpful for routine orientation mapping and in-situ deformation studies in both academic and industrial contexts.
dc.description.noteOctober 2025
dc.identifier.urihttp://hdl.handle.net/1993/39096
dc.language.isoeng
dc.subjectHollow Cone Dark Field Imaging
dc.subjectAutomatic Acquisition
dc.subjectMultislice simulation framework
dc.subjectMagnesium
dc.subjectContrast
dc.titleHollow cone dark field imaging: automatic acquisition, and its contrast for magnesium
local.subject.manitobano
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